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Manufacturer supply top purity Methyl 2-bromobenzoate 610-94-6 with GMP standards
- Molecular Formula: C8H7BrO2
- Molecular Weight: 215.046
- Appearance/Colour: Colorless or light yellow transparent liquid
- Vapor Pressure: 0.0368mmHg at 25°C
- Melting Point: 252°C
- Refractive Index: n20/D 1.559(lit.)
- Boiling Point: 241 °C at 760 mmHg
- Flash Point: 99.6 °C
- PSA： 26.30000
- Density: 1.498 g/cm3
- LogP: 2.23570
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610-94-6 Process route
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67-56-1
methanol
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7154-66-7
2-bromobenzoic acid chloride
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-
610-94-6
2-bromobenzoic acid methyl ester
| Conditions | Yield |
|---|---|
|
|
|
|
With
triethylamine;
In
dichloromethane;
at 0 ℃;
|
|
|
With
sulfuric acid;
for 4h;
Reflux;
|
-
-
67-56-1
methanol
-
-
88-65-3
2-bromobenzoic-acid
-
-
610-94-6
2-bromobenzoic acid methyl ester
| Conditions | Yield |
|---|---|
|
With
sulfuric acid;
Reflux;
Inert atmosphere;
|
99%
|
|
With
sulfuric acid;
Reflux;
|
99%
|
|
With
sulfuric acid;
at 0 ℃;
for 20.25h;
Reflux;
|
96%
|
|
With
sulfuric acid;
for 0.25h;
Reflux;
Microwave irradiation;
|
95%
|
|
With
thionyl chloride;
at 90 ℃;
for 4h;
Cooling with ice;
|
95%
|
|
With
sulfuric acid;
for 11h;
Reflux;
|
95%
|
|
With
sulfuric acid;
at 0 ℃;
for 18h;
Reflux;
|
95%
|
|
With
sulfuric acid;
at 0 ℃;
for 18h;
Inert atmosphere;
Reflux;
|
93%
|
|
With
chloro-trimethyl-silane;
for 8h;
Heating / reflux;
|
92%
|
|
With
sulfuric acid;
for 5h;
Reflux;
|
92%
|
|
With
sulfuric acid;
at 0 ℃;
for 16h;
Reflux;
|
83%
|
|
With
Oxone;
In
toluene;
at 60 ℃;
for 48h;
Green chemistry;
|
81%
|
|
sulfuric acid;
|
80%
|
|
With
sulfuric acid;
for 1h;
Reflux;
|
64%
|
|
With
sulfuric acid;
for 1h;
Reflux;
|
64%
|
|
With
hydrogenchloride;
|
|
|
With
sulfuric acid;
Reflux;
|
|
|
Acidic conditions;
Reflux;
|
|
|
Reflux;
Acidic conditions;
|
|
|
With
sulfuric acid;
|
|
|
Acidic conditions;
Reflux;
|
|
|
With
sulfuric acid;
|
|
|
With
thionyl chloride;
|
|
|
Acidic conditions;
|
|
|
With
sulfuric acid;
for 2h;
Inert atmosphere;
Reflux;
|
|
|
With
sulfuric acid;
for 24h;
Reflux;
|
|
|
With
sulfuric acid;
for 5h;
Reflux;
|
|
|
2-bromobenzoic-acid;
With
thionyl chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
Schlenk technique;
methanol;
In
dichloromethane;
Inert atmosphere;
Schlenk technique;
|
|
|
With
sulfuric acid;
Reflux;
|
|
|
With
sulfuric acid;
for 11h;
Reflux;
|
|
|
With
thionyl chloride;
at 40 ℃;
for 1h;
|
|
|
With
sulfuric acid;
for 8h;
Reflux;
|
610-94-6 Upstream products
-
67-56-1
methanol
-
7154-66-7
2-bromobenzoic acid chloride
-
88-65-3
2-bromobenzoic-acid
-
108-86-1
bromobenzene
610-94-6 Downstream products
-
7073-69-0
2-(2-bromophenyl)propanol
-
59346-13-3
((2-bromophenyl)chloromethylene)dibenzene
-
61593-02-0
1-(2'-bromophenyl)-1,1-diphenylmethanol
-
859946-42-2
2-bromo-4',4''-dichloro-trityl chloride
